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Supervisor：Jiangxi University Of Science And Technology
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Jiangxi Nonferrous Metals Society
ISSN：1674-9669
CN：36-1311/TF
CODEN YJKYA9
Volume 8 Issue 6
Dec.  2017
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ZHAO Fei, LI Juan. Determination of hydrogen content of hafnium by inert gas fusion infrared method[J]. Nonferrous Metals Science and Engineering, 2017, 8(6): 117-120. DOI: 10.13264/j.cnki.ysjskx.2017.06.019
Citation: ZHAO Fei, LI Juan. Determination of hydrogen content of hafnium by inert gas fusion infrared method[J]. Nonferrous Metals Science and Engineering, 2017, 8(6): 117-120. DOI: 10.13264/j.cnki.ysjskx.2017.06.019
shu

Determination of hydrogen content of hafnium by inert gas fusion infrared method

  • Western Metal Materials Co. Ltd., Xi'an 710016, China

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  • Received Date: July 26, 2017
  • Published Date: December 30, 2017
    Graphical Abstract
    • Abstract
  • Using LECO-NH836 nitrogen-hydrogen analyzer, the sample was melted in an inert atmosphere, and the content of hydrogen in hafnium was detected by the infrared method. By choosing 1.00 g nickel basket as the flux of hydrogen release in hafnium, the influence of different analytical powers on the hydrogen content analysis was studied. The analysis power of 5 000 W, the shortest analysis time of 60 s, and the sample mass of 0.10 g were selected to verify the applicability of titanium reference materials.The RSDs of 11 replicates of the two samples were 5.64 % and 1.52 %, respectively, with good precision.The spiked recoveries ranged from 95.18 % to 105.26 %. The result of the study is instructive for the accurate determination of hydrogen in hafnium.
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    • References (24)
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