Current Issue Cover
Advanced Search
Founded in 1987， Bimonthly
Supervisor：Jiangxi University Of Science And Technology
Sponsored by：Jiangxi University Of Science And Technology
Jiangxi Nonferrous Metals Society
ISSN：1674-9669
CN：36-1311/TF
CODEN YJKYA9
Volume 19 Issue 4
Dec.  2005
Turn off MathJax
Article Contents
Abstract
References
Related Articles
LIAN Ping, LI Lei, YANG Yan-chao, WANG Ke-jun, LI Yong-xiu. Catalytic Synthesis of Sucrose Fatty Acid Ester with Rare Earth Solid Super Acid by Microwave Irradiation[J]. Nonferrous Metals Science and Engineering, 2005, 19(4): 36-39.
Citation: LIAN Ping, LI Lei, YANG Yan-chao, WANG Ke-jun, LI Yong-xiu. Catalytic Synthesis of Sucrose Fatty Acid Ester with Rare Earth Solid Super Acid by Microwave Irradiation[J]. Nonferrous Metals Science and Engineering, 2005, 19(4): 36-39.
shu

Catalytic Synthesis of Sucrose Fatty Acid Ester with Rare Earth Solid Super Acid by Microwave Irradiation

  • 1.

    Department of Chemistry, Nanchang University, Nanchang 330047, Jiangxi, China

  • 2.

    Department of Chemistry and Life Science, Gannan Teachers' College, Ganzhou 341000, Jiangxi, China

  • 3.

    College of Biological and Chemical Engineering, Jiaxing University, Jiaxing 314001, Zhejiang, China

More Information
  • Received Date: November 29, 2005
  • Published Date: December 30, 2005
    Graphical Abstract
    • Abstract
  • The syntheses of sucrose fatty acid ester catalyzed by rare earth solid super acid under microwave irradiation is investigated, including the influences of microwave power, radiation time, catalyst and emulsifier on the reaction. The results shows that the catalytic activity of Gd3+-SO42-/ZrO2、Y3+-SO42-/ZrO2 is better than K2CO3 when microwave power is 390W and radiation time is 20min, and the reaction time of synthesis is shortened from 4~8h in traditional heating menthol to 20min under microwave irradiation.
    • FullText(HTML)
    • References (7)
  • [1]
    李尊江, 邢德娜.蔗糖脂肪酸酯的制备应用及发展[J].精细石油化工进展.2003, 4(5):16-18. http://www.cqvip.com/qk/82128X/200305/7911073.html
    [2]
    章亚东, 蒋登高, 刘诗飞, 等.无溶剂法合成蔗糖硬脂酸酯的工艺研究[J].四川大学学报, 2002, 34(5):67-71. http://www.docin.com/p-527863172.html
    [3]
    吴谋成, 刘志伟.蔗糖脂肪酸酯的水化法合成工艺研究[J].华中农业大学学报, 1997, 16(4):399-404. http://www.cqvip.com/qk/90088X/199704/2638305.html
    [4]
    崔秀兰, 郭海福, 林明丽, 等.镧改性固体超强酸SO42-/ ZrO2- TiO2/La3+催化剂的制备及性能研究[J].中国稀土学报, 2003, 21(4):460-464. http://www.whxb.pku.edu.cn/CN/abstract/abstract22575.shtml
    [5]
    George M, Rodgers H. Application of microwave-accelerated organic synthesis[J]. Radiat. Phys.Chem., 1995, 45(4): 567-579. doi: 10.1016/0969-806X(94)00071-Q
    [6]
    练萍, 杨衍超.稀土固体超强酸Gd3+-SO42-/ZrO2催化剂的制备及表征[J].赣南师范学院学报, 2005, (3):50-51. http://www.whxb.pku.edu.cn/CN/abstract/abstract22573.shtml
    [7]
    刘志伟.蔗糖酯粗品的纯化工艺研究[J].武汉工业学院学报, 1999, (3):11-14. http://www.cqvip.com/QK/96738A/199903/3650579.html
    • Related Articles

  • Related Articles

    [1]LIAO Bin, LIU Fupeng. Extraction behavior of germanium in different leaching systems from zinc oxide dust[J]. Nonferrous Metals Science and Engineering, 2023, 14(5): 597-605. DOI: 10.13264/j.cnki.ysjskx.2023.05.001
    [2]HUANG Chengge, TANG Daowen, CAI Pengyuan, XIONG Huakang, HUANG Biao. Orthogonal test on the leaching of a refractory gold ore in Guizhou province by bleaching powder[J]. Nonferrous Metals Science and Engineering, 2020, 11(2): 97-103. DOI: 10.13264/j.cnki.ysjskx.2020.02.014
    [3]ZHAO Tianyu, SONG Yunfeng, LI Yongli, ZHAO Zhongwei, HE Lihua, CHEN Xingyu, LIU Xuheng. Recovery of lithium from leaching solution of anode materials in waste lithium-ion batteries by solvent extraction method[J]. Nonferrous Metals Science and Engineering, 2019, 10(1): 49-53. DOI: 10.13264/j.cnki.ysjskx.2019.01.008
    [4]Zhang Ying, Zhang Ting-an. Research progress for vanadium extraction from vanadium leach solution by solvent extraction[J]. Nonferrous Metals Science and Engineering, 2017, 8(5): 14-20. DOI: 10.13264/j.cnki.ysjskx.2017.05.002
    [5]ZHANG Ying, ZHANG Ting'an. Extraction of vanadium from the leaching solution from convertervanadium slag without roasting using N1923[J]. Nonferrous Metals Science and Engineering, 2015, 6(6): 14-19. DOI: 10.13264/j.cnki.ysjskx.2015.06.003
    [6]HUANG Jiaquan, WANG Yaping, WANG Huatai, PENG Tangjian, WU Xueling, ZHOU H ongbo, ZENG Weimin. Sulphuric acid leaching of Yulong oxide copper ore based on orthogonal design test[J]. Nonferrous Metals Science and Engineering, 2014, 5(5): 123-129. DOI: 10.13264/j.cnki.ysjskx.2014.05.023
    [7]ZHAO Mu-yue, WANG Fu-sheng, SUN Zhi-yu. Review of W-base high proportion alloy's development in China[J]. Nonferrous Metals Science and Engineering, 2013, 4(5): 1-5. DOI: 10.13264/j.cnki.ysjskx.2013.05.016
    [8]WU Zai-jiu. Recovery of gold, silver and copper from complex gold concentrate by roasting-acidic leaching-cyanidation process[J]. Nonferrous Metals Science and Engineering, 2013, 4(2): 25-29. DOI: 10.13264/j.cnki.ysjskx.2013.02.008
    [9]LIU Xiao-yan, LI Jian, LV Yu-guo. Determination of Additives in Copper Electrolyte[J]. Nonferrous Metals Science and Engineering, 2008, 22(3): 22-25.
    [10]ZHOU Peng, CHENG Pei-yuan. The Additives and the Magnetic Properties of Permanent Ferrite[J]. Nonferrous Metals Science and Engineering, 2007, 21(1): 27-29.

Catalog

    Get Citation
    PDF
    XML

    Article Metrics

    Article views (104) PDF downloads (2) Cited by()
    Related

    Copyright © 2010 Editorial Department of Nonferrous Metals Science and Engineering All rights reserved

    Address：11th floor, bishop building, University of science and technology, No. 86, Hongqi Avenue, Ganzhou City, Jiangxi Province  Tel：0797-8312555

    Supported by: Beijing Renhe Information Technology Co., Ltd.  Baidu Analytics

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return