Synthesis of Ni-Ti composite powder by radio frequency plasma spheroidization process

XU Ping; LIU Danhua; HU Jie; LIN Gaoyong

doi:10.13264/j.cnki.ysjskx.2020.01.011

Volume 11 Issue 1

Feb. 2020

Turn off MathJax

Article Contents

Abstract

References

Nonferrous Metals Science and Engineering > 2020 > 39(1): 67-71. > DOI: 10.13264/j.cnki.ysjskx.2020.01.011

XU Ping, LIU Danhua, HU Jie, LIN Gaoyong. Synthesis of Ni-Ti composite powder by radio frequency plasma spheroidization process[J]. Nonferrous Metals Science and Engineering, 2020, 39(1): 67-71. DOI: 10.13264/j.cnki.ysjskx.2020.01.011

Citation:

PDF (1567 KB)

Synthesis of Ni-Ti composite powder by radio frequency plasma spheroidization process

XU Ping^{1, 2},
LIU Danhua²,
HU Jie²,
LIN Gaoyong^2, ,

1.
School of Materials Science and Engineering, Central South University, Changsha 410083, China
2.
Guangdong Institute of Materials and Processing, Guangdong Academy of Sciences, Guangzhou 510650, China

More Information

Received Date: August 07, 2019
Published Date: February 28, 2020

Graphical Abstract

Abstract

Abstract

Near-equiatomic Ni-Ti composite powder was synthesized by using gas atomized Ni powder and irregularly shaped Ti powder by TEKNA radio frequency plasma spheroidization process. The effect of carrier gas flow rate on the morphology, particle size, phase distribution and element distribution of the prepared powder was investigated. The morphology and particle size of the power were characterized by scanning electron microscopy and particle size analyzer while the phase constitution and element distribution were characterized by XRD and EDS. The results showed that compared with original powder, the prepared powder had a significant increase in particle size; as the carrier gas flow rate increased, so did Ni content of the powder. And when the carrier gas flow rate was 2.5 L/min, the spheroidization rate reached 100% and the Ni mass fraction was 55.2%; the spheroidized powder consisted of three phases, namely Ni phase, Ti phase and NiTi phase; Ni and Ti elements could be observed in each particle of the power, but the mass fraction of Ti and Ni contained in each particle was not completely the same.
- RF plasma,
- carrier gas flow rate,
- Ni-Ti composite powder,
- element distribution

FullText(HTML)

References (23)

References

[1]	WALKER J M, HABERLAND C, TAHERI M, et al. Process development and characterization of additively manufactured nickel-titanium shape memory parts[J]. Journal of Intelligent Material Systems and Structures, 2016, 27(19): 2653-2660. doi: 10.1177/1045389X16635848
[2]	SHEN L, CHEN G, ZHAO S, et al. Properties and microstructures of spherical NiTi powders prepared by plasma rotating electrode process[J]. Materials Science & Engineering of Powder Metallurgy, 2017, 22(4): 539-545. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=fmyjclkxygc201704013
[3]	ELAHINIA M H, HASHEMI M, TABESH M, et al. Manufacturing and processing of NiTi implants: A review[J]. Progress in Materials Science, 2012, 57(5): 911-946. doi: 10.1016/j.pmatsci.2011.11.001
[4]	YABLOKOVA G, SPEIRS M, VAN J, et al. Rheological behavior of β-Ti and NiTi powders produced by atomization for SLM production of open porous orthopedic implants[J]. Powder Technology, 2015, 283: 199-209. doi: 10.1016/j.powtec.2015.05.015
[5]	HAMILTON R F, BIMBER B A, TAHERI M, et al. Multi-scale shape memory effect recovery in NiTi alloys additive manufactured by selective laser melting and laser directed energy deposition[J]. Journal of Materials Processing Technology, 2017, 250: 55-64. doi: 10.1016/j.jmatprotec.2017.06.027
[6]	黄卫东, 吕晓卫, 林鑫, 等.激光成形制备生物医用材料研究现状与发展趋势[J].中国材料进展, 2011, 30(4): 1-10. http://d.old.wanfangdata.com.cn/Periodical/zgcljz201104001
[7]	SHEN L, ZHAO S. Properties and microstructures of spherical NiTi powders prepared by plasma rotating electrode process[J]. Materials Science & Engineering of Powder Metallurgy, 2017, 22(4): 539-545. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=fmyjclkxygc201704013
[8]	杨全占, 魏彦鹏, 高鹏, 等.金属增材制造技术及其专用材料研究进展[J].材料导报, 2016(1): 107-111.
[9]	金莹, 刘平, 史金光, 等.雾化压力对电极感应熔炼气雾化TC₄粉末形貌与性能的影响[J].粉末冶金材料科学与工程, 2018, 23(3): 312-317. doi: 10.3969/j.issn.1673-0224.2018.03.012
[10]	张飞, 高正江.增材制造用金属粉末材料及其制备技术[J].工业技术创新, 2017(4): 63-67. http://d.old.wanfangdata.com.cn/Periodical/gyjscx201704012
[11]	沈垒, 陈刚, 赵少阳, 等. PREP法制备球形NiTi合金粉末的特性及显微组织[J].粉末冶金材料科学与工程, 2017(4): 539-543. doi: 10.3969/j.issn.1673-0224.2017.04.013
[12]	王建军, 郝俊杰, 郭志猛, 等.射频等离子体制备球形粉末的数值模拟[J].中国科技论文, 2015, 10(22): 2642-2647. doi: 10.3969/j.issn.2095-2783.2015.22.014
[13]	王运锋.射频等离子体制备球形TC₄钛合金粉[J].钛工业进展, 2013(6): 44-44. http://d.old.wanfangdata.com.cn/Periodical/tgyjz201306021
[14]	王辉, 陈再良.形状记忆合金材料的应用[J].机械工程材料, 2002(3): 5-8. doi: 10.3969/j.issn.1000-3738.2002.03.002
[15]	LI R, QIN M, HUANG H, et al. Fabrication of fine-grained spherical tungsten powder by radio frequency (RF) inductively coupled plasma spheroidization combined with jet milling[J]. Advanced Powder Technology, 2017, 28(12): 3158-3163. doi: 10.1016/j.apt.2017.09.019
[16]	WEI W H, WANG L Z, CHEN T, et al. Study on the flow properties of Ti-6Al-4V powders prepared by radio-frequency plasma spheroidization[J]. Advanced Powder Technology, 2017, 28(9): 2431-2437. doi: 10.1016/j.apt.2017.06.025
[17]	HAO Z, FU Z, LIU J, et al. Spheroidization of a granulated molybdenum powder by radio frequency inductively coupled plasma[J]. International Journal of Refractory Metals and Hard Materials, 2019, 82: 15-22. doi: 10.1016/j.ijrmhm.2019.03.023
[18]	王建军, 郝俊杰, 郭志猛.射频等离子体制备球形铌粉[J].粉末冶金材料科学与工程, 2014(5): 361-366. http://d.old.wanfangdata.com.cn/Periodical/fmyjclkxygc201403005
[19]	黎英, 刘鸿.电感耦合等离子发射光谱法测定稀土精矿中钍量[J].有色金属科学与工程, 2010, 1(6): 86-88. http://ysjskx.paperopen.com/oa/DArticle.aspx?type=view&id=201304010
[20]	谢璐, 刘鸿, 杨峰.某钨矿山土壤中重金属元素测定[J].有色金属科学与工程, 2015, 6(5): 124-128. http://ysjskx.paperopen.com/oa/DArticle.aspx?type=view&id=201505023
[21]	ZHANG H, BAI L, HU P, et al. Single-step pathway for the synthesis of tungsten nanosized powders by RF induction thermal plasma[J]. International Journal of Refractory Metals and Hard Materials, 2012, 31: 33-38. doi: 10.1016/j.ijrmhm.2011.09.002
[22]	LU X, ZHU L P, ZHANG B, et al. Simulation of flow field and particle trajectory of radio frequency inductively coupled plasma spheroidization[J]. Computational Materials Science, 2012, 65: 13-18. doi: 10.1016/j.commatsci.2012.06.008
[23]	KOBAYASHI N, KAWAKAMI Y, KAMADA K, et al. Spherical submicron-size copper powders coagulated from a vapor phase in RF induction thermal plasma[J]. Thin Solid Films, 2008, 516(13): 4402-4406. doi: 10.1016/j.tsf.2007.10.064

[1]	LIAN Baidong, QIAO Dengpan, YANG Tianyu, WANG Jun, CHEN Jian, LI Shaoteng, LI Yongming, GAO Bo, LONG Gan. Research on pipeline transportation design of tailings slurry from a tin mine in Yunnan Province based on ANSYS-FLUENT[J]. Nonferrous Metals Science and Engineering, 2024, 15(3): 407-421. DOI: 10.13264/j.cnki.ysjskx.2024.03.011
[2]	GUO Hao, WANG Yajie, ZHAO Hongbo, ZUO Haibin. Numerical simulation of pulverized coal forming process[J]. Nonferrous Metals Science and Engineering, 2024, 15(3): 357-363. DOI: 10.13264/j.cnki.ysjskx.2024.03.006
[3]	LIU Zheng, ZHANG Jiayi, DENG Keyue. Numerical simulation of aluminum molten liquid and its particle trajectories in electromagnetic field based on Fluent[J]. Nonferrous Metals Science and Engineering, 2015, 6(4): 46-51. DOI: 10.13264/j.cnki.ysjskx.2015.04.010
[4]	CHENG Qiuting, DENG Fei, CHEN Yanhong, XIA Yijiang, WANG Xiaojun. Numerical simulation analysis on the stability of mined-out area[J]. Nonferrous Metals Science and Engineering, 2015, (2): 85-88. DOI: 10.13264/j.cnki.ysjskx.2015.02.016
[5]	ZHAO Kui, SHAO Hai, XU Feng, ZENG Peng, DENG Xiao-ping, WANG Ming. Numerical simulation of stability of mining of different mining entrances in a copper mine[J]. Nonferrous Metals Science and Engineering, 2013, 4(2): 46-50. DOI: 10.13264/j.cnki.ysjskx.2013.02.009
[6]	WU Hui, CAI Si-jing, WANG Zhang, CHEN Wu-jiu. Numerical simulation of ventilation network and its validation in Hemushan iron mine[J]. Nonferrous Metals Science and Engineering, 2012, 3(3): 60-65. DOI: 10.13264/j.cnki.ysjskx.2012.03.013
[7]	RAO Yun-zhang, CHEN Hui, XIAO Guang-zhe, CHEN Guo-liang. On the Design of Stope Bottom Structures Based on FLAC 3D Numerical Simulation[J]. Nonferrous Metals Science and Engineering, 2011, 2(2): 43-47. DOI: 10.13264/j.cnki.ysjskx.2011.02.009
[8]	XU Cong-wu, ZHAO Kui, XIE Dao-hui. Numerical Simulation Research on Tunnel Arrangement in Schistosity Rock[J]. Nonferrous Metals Science and Engineering, 2008, 22(3): 6-8.
[9]	CUI Dong-liang, LI Xi-bing, ZHAO Guo-ya. Analysis of the Numerical Simulation to Structure Parameter of Hard-To-Mine Ore Body in Xincheng Gold Mine[J]. Nonferrous Metals Science and Engineering, 2006, 20(3): 13-17.
[10]	QIAO Jun-yu, XU Guo-yuan. Numerical Simulation in Reinforcement for Deep Foundation Pit with Soil Nailing[J]. Nonferrous Metals Science and Engineering, 2005, 19(4): 24-24.

Cited By

Get Citation

PDF

XML

Article Metrics

Article views (74) PDF downloads (3)

Synthesis of Ni-Ti composite powder by radio frequency plasma spheroidization process

Abstract

References

Related Articles

Catalog

Article Metrics

Related

Synthesis of Ni-Ti composite powder by radio frequency plasma spheroidization process

Abstract

References

Related Articles

Catalog

Article Metrics

Related

Export File

Citation

Format

Content