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Founded in 1987， Bimonthly
Supervisor：Jiangxi University Of Science And Technology
Sponsored by：Jiangxi University Of Science And Technology
Jiangxi Nonferrous Metals Society
ISSN：1674-9669
CN：36-1311/TF
CODEN YJKYA9
Volume 14 Issue 3
Jun.  2023
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ZHOU Wenwang, JIANG Chenxi, ZENG Danliang, WU Yibo, QIU Tingsheng, YU Wen. Study on preparation of MoSx@ZVI composite by carbothermal reduction synthesis and its treatment of acid orange G wastewater[J]. Nonferrous Metals Science and Engineering, 2023, 14(3): 407-415. DOI: 10.13264/j.cnki.ysjskx.2023.03.014
Citation: ZHOU Wenwang, JIANG Chenxi, ZENG Danliang, WU Yibo, QIU Tingsheng, YU Wen. Study on preparation of MoSx@ZVI composite by carbothermal reduction synthesis and its treatment of acid orange G wastewater[J]. Nonferrous Metals Science and Engineering, 2023, 14(3): 407-415. DOI: 10.13264/j.cnki.ysjskx.2023.03.014
shu

Study on preparation of MoSx@ZVI composite by carbothermal reduction synthesis and its treatment of acid orange G wastewater

  • a.

    School of Resources and Environmental Engineering, Jiangxi University of Science and Technology, Ganzhou 34000, Jiangxi, China

  • b.

    School of Emergency Management and Safety Engineering, Jiangxi University of Science and Technology, Ganzhou 34000, Jiangxi, China

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  • Received Date: November 21, 2022
  • Revised Date: December 25, 2022
  • Available Online: June 30, 2023
    Graphical Abstract
    • Abstract
  • MoSx@ZVI composite was synthesized with molybdenite (MoS2), limonite and anthracite by carbothermal reduction. Effects of molybdenite dosage, roasting temperature, anthracite content, and roasting time on the performance of the prepared MoSx@ZVI for removing orange G (OG) were investigated. MoSx@ZVI with the best performance was prepared by roasting at 1 000 ℃ for 60 min with 6% of molybdenum and 25% anthracite. MoSx@ZVI prepared under the best conditions was analyzed by X-ray diffraction, scanning electron microscopy and energy dispersive spectrometry. The results show that a large amount of sulfide zero-valent iron with a core-shell structure is formed in the material, the core is Fe-Mo-C alloy, and the shell may be composed of molybdenum sulfide, FeS, C, molybdenum oxide and iron oxide. The degradation experiment results show that the removal rate of OG is above 90% when MoSx@ZVI prepared under the optimal conditions is crushed to particle size smaller than 0.1 mm, and 400 mL OG simulated wastewater with a concentration of 200 mg/L is treated with 0.6 g of MoSx@ZVI for 150 min within the initial pH range of 3.0-10.0.
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    • References (43)
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