Founded in 1987, Bimonthly
Supervisor:Jiangxi University Of Science And Technology
Sponsored by:Jiangxi University Of Science And Technology
Jiangxi Nonferrous Metals Society
ISSN:1674-9669
CN:36-1311/TF
CODEN YJKYA9
LONG Haizhen, WANG Jingfeng, WANG Maosheng, KONG Huimin. Determination of silver content in zinc anode slime by fire assay gravimetry method[J]. Nonferrous Metals Science and Engineering, 2019, 10(6): 76-80. DOI: 10.13264/j.cnki.ysjskx.2019.06.012
Citation: LONG Haizhen, WANG Jingfeng, WANG Maosheng, KONG Huimin. Determination of silver content in zinc anode slime by fire assay gravimetry method[J]. Nonferrous Metals Science and Engineering, 2019, 10(6): 76-80. DOI: 10.13264/j.cnki.ysjskx.2019.06.012

Determination of silver content in zinc anode slime by fire assay gravimetry method

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  • Received Date: June 11, 2019
  • Published Date: December 30, 2019
  • In this paper, a method for determination of silver content in zinc anode mud by concentration of fire test gold is studied.Rich in silver by lead, form a lead buckle, to remove lead at suitable temperatures, when ash blows, lead oxidizes to lead oxide and penetrates a porous ash dish to remove lead and impurities, Silver is not oxidized and remains in the ash dish to form silver particles.Silver grain quality obtained by weighing method, Silver grain mass minus lead oxide blank silver mass is the amount of silver.The method does not require a second trial and has high efficiency, low cost, accurate results and good reproducibility, ability to direct production quickly and accurately, Suitable for modern enterprise production, This method can be used for the determination of the silver content in zinc anode mud 50 ~ 1000 g/t.
  • [1]
    矿产资源工业要求手册编委会.矿产资源工业要求手册[M].北京:地质出版社, 2014:203-210.
    [2]
    铅阳极泥化学分析方法: 金量和银量的测定: 火法冶炼, YS/T 775.5—2011[S].
    [3]
    梁金凤, 王景凤.火试金重量法测定铅阳极泥中银含量方法的改进[C]//2014国际冶金及材料分析测试学术报告会论文集.北京: 中国金属学会, 2014, 34: 314-317.
    [4]
    王景凤.火试金重量法测定金精矿中金银含量方法的改进[J].有色矿冶, 2007, 33(1):58-60.
    [5]
    王景凤.火试金富集测定粗铅中金、银含量的改进试验研究[J].有色金属科学与工程, 2018, 9(3):100-104. http://ysjskx.paperopen.com/oa/DArticle.aspx?type=view&id=2018010021
    [6]
    王景凤, 张瑾, 董哲飞.青海某高硅复杂金矿石中金银含量测定方法研究[J].有色金属科学与工程, 2018, 9(6):89-93. http://ysjskx.paperopen.com/oa/DArticle.aspx?type=view&id=201806014
    [7]
    王景凤, 王茂盛, 董哲飞, 等.复杂矿石中银的测定[J].有色矿冶, 2017, 33(5):51-53. doi: 10.3969/j.issn.1007-967X.2017.05.014
    [8]
    冯振华, 王可伟.火焰原子吸收光谱法直接测定锡阳极泥中的银[J].中国无机分析化学, 2017, 7(2):59-62. doi: 10.3969/j.issn.2095-1035.2017.02.015
    [9]
    雷素函, 冯静弦.火焰原子吸收光谱法测定铅冶炼渣中的银量[J].中国无机分析化学, 2013, 3(B10):62-64. http://d.old.wanfangdata.com.cn/Periodical/zgwjfxhxwz2013z1022
    [10]
    金精矿化学分析方法银量的测定湿法冶炼, GB/T 7739.2—2007[S].
    [11]
    铜矿石、铅矿石和锌矿石化学分析方法: 银量测定: 湿法冶炼, GB/T 14353.11—2010[S].
    [12]
    魏雅娟, 吴雪英, 江荆, 等.微波消解-电感耦合等离子体原子发射光谱法测定银精矿中铅锌铜砷锑铋镉[J].冶金分析, 2018, 38(5):47-53. http://d.old.wanfangdata.com.cn/Periodical/yjfx201805009
    [13]
    刘溢锋, 冯俊汉, 李展江, 等.电感耦合等离子体发射光谱法同时测定粗铜中的金和银[J].冶金分析, 2012, 32(7):52-54. doi: 10.3969/j.issn.1000-7571.2012.07.011
    [14]
    周西林, 张宏, 王亚森, 等.电感耦合等离子体原子发射光谱法测定铝合金中银[J].冶金分析, 2013, 33(4):64-67. doi: 10.3969/j.issn.1000-7571.2013.04.012
    [15]
    铅精矿化学分析方法: 银量和金量的测定火法冶炼, GB/T 8152.10—2006[S].
    [16]
    铜精矿化学分析方法: 金和银量的测定: 火法冶炼, GB/T 3884.2—2012[S].
    [17]
    锌精矿化学分析方法: 金和银含量的测定火法冶炼, GB/T 8151.19—2012[S].
    [18]
    冰铜化学分析方法: 金量和银量的测定: 火法冶炼, YS/T 990.2—2014[S].
    [19]
    粗铅化学分析方法: 金量和银量的测定: 火法冶炼, YS/T 248.6—2007[S].
    [20]
    铜阳极泥化学分析方法: 金量和银量的测定: 火法冶炼, YS/T 745.2—2010[S].
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