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ISSN：1674-9669
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CODEN YJKYA9
Volume 10 Issue 3
Jun.  2019
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LI Wei, ZHANG Xiaolin, NING Rui. Experimental study on thallium removal from ammonium perrhenate[J]. Nonferrous Metals Science and Engineering, 2019, 10(3): 21-25. DOI: 10.13264/j.cnki.ysjskx.2019.03.004
Citation: LI Wei, ZHANG Xiaolin, NING Rui. Experimental study on thallium removal from ammonium perrhenate[J]. Nonferrous Metals Science and Engineering, 2019, 10(3): 21-25. DOI: 10.13264/j.cnki.ysjskx.2019.03.004
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Experimental study on thallium removal from ammonium perrhenate

  • Daye Nonferrous Metals Co., Ltd., Huangshi 435005, China

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  • Received Date: March 19, 2019
  • Published Date: June 29, 2019
    Graphical Abstract
    • Abstract
  • Ammonium perrhenate extracted from copper smelting acid contains a certain amount of Tl element which affects the quality of ammonium perrhenate and limits the end application of rhenium products. In this paper, a traditional adsorption method was used to remove Tl: activated carbon, TiO2, KI and XH30 resin were used to carry out static absorption tests. On this basis, the effects of rhenium solution concentration, adsorption linear velocity and rhenium solution pH on the dynamic adsorption of Tl by using XH30 resin were investigated. The results showed that the adsorption effect on Tl by using activated carbon and KI was not ideal, and the adsorption rates of Tl by using TiO2 and XH30 resin for long-term dynamic adsorption were 96.9 % and 97.95 %, respectively. Tl was adsorbed with XH30 resin column. When [Re] was 10 g/L, [Tl], roughly 5 mg/L, pH, 8.5, and linear velocity of adsorption, controlled at 8 cm/min, the Tl removal rate could stand stable at 93.4 % and the grade of recrystallized ammonium perrhenate remained above 99.99 %.
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    • References (20)
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