Founded in 1987, Bimonthly
Supervisor:Jiangxi University Of Science And Technology
Sponsored by:Jiangxi University Of Science And Technology
Jiangxi Nonferrous Metals Society
ISSN:1674-9669
CN:36-1311/TF
CODEN YJKYA9
WANG Jingfeng, ZHANG Jin, DONG Zhefei. Determination method of gold and silver content in a high silicon complex gold ore in Qinghai[J]. Nonferrous Metals Science and Engineering, 2018, 9(6): 89-93. DOI: 10.13264/j.cnki.ysjskx.2018.06.014
Citation: WANG Jingfeng, ZHANG Jin, DONG Zhefei. Determination method of gold and silver content in a high silicon complex gold ore in Qinghai[J]. Nonferrous Metals Science and Engineering, 2018, 9(6): 89-93. DOI: 10.13264/j.cnki.ysjskx.2018.06.014

Determination method of gold and silver content in a high silicon complex gold ore in Qinghai

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  • Received Date: July 02, 2018
  • Available Online: January 27, 2022
  • Published Date: December 30, 2018
  • There is no standard method for the determination of gold and silver in gold ore. Generally, it is based on the classical determination method of gold in gold concentrate, GB/T 7739.1-2007. When this method is used to determine gold ore samples containing higher silica, it is melted in fire. During the process, the melt easily overflows and causes the test to fail. At the same time, because the sample contains a small amount of silver, the ratio of the amount of silver to the amount of gold in the formed gold-silver granules is very different, which brings great difficulty to the gold-splitting process. It is not even effective to separate. Based on this, in response to the national call for energy conservation, emission reduction and consumption reduction, according to the nature of the samples, the research was carried out through experiments, and the suitable test conditions for the slag lead buckle were optimized and established by continuously changing the amount of solid flux. By adding sterling silver, it compensates for the proportion of silver and gold in the sample. It has been verified under optimized working conditions, the analysis results are accurate and fast, the environmental pollution caused by repeated slag reduction is reduced, the labor intensity and difficulty are reduced, the detection cost is greatly reduced, and it has been used in a large number of high-silicon complex gold ore gold. The silver content was measured and achieved good results. The method is applicable to the determination of gold content in gold ore: 100~600 g/t, and silver amount: 30~100 g/t.
  • [1]
    刘亚溪.电感耦合等离子体发射光谱法测定锑金精矿中的金[J].化工管理, 2017(11):122-124. doi: 10.3969/j.issn.1008-4800.2017.11.109
    [2]
    贺秀珍, 钟清慎, 马玉天, 等.复杂金精矿矿物特性及焙烧预处理工艺研究[J].有色金属(冶炼部分), 2014(8):38-41. doi: 10.3969/j.issn.1007-7545.2014.08.010
    [3]
    李廷梁.俄罗斯难浸金矿的生物冶金技术[J].贵金属, 1998, 19(1):54-56. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=QK199801019362
    [4]
    许鹏秋.难浸金矿石采用Polycom高压辊磨矿的进展[J].国外黄金参考, 1997(3):8-13. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=QK199701068142
    [5]
    张永涛.中国黄金矿产资源开发及矿产品供需形势分析[J].中国矿业, 2009, 18(8):8-11. http://d.old.wanfangdata.com.cn/Periodical/zgky200902003
    [6]
    张秋荣, 张海芹, 陈文宾.5-(对羧基苯偶氮)8-羟基喹哪啶分光光度法测定痕量金[J].冶金分析, 2011, 31(1):70-73. doi: 10.3969/j.issn.1000-7571.2011.01.015
    [7]
    刘涛, 李念占, 张汝生.封闭溶样氢醌容量法测定焙烧矿样中的金[J].黄金, 2007, 28(11):49-50. doi: 10.3969/j.issn.1001-1277.2007.11.014
    [8]
    薛光, 赵玉娥.金测定方法的最新进展(待续)[J].黄金, 2007, 28(1):51-54. doi: 10.3969/j.issn.1001-1277.2007.01.013
    [9]
    成勇, 袁金红, 肖军, 等.微波消解-电感耦合等离子体质谱法(ICP-MS)测定矿石中金和银[J].中国无机分析化学, 2012(1):51-54. doi: 10.3969/j.issn.2095-1035.2012.01.0011
    [10]
    赵延庆.聚氨酯泡沫塑料吸附-电感耦合等离子体质谱法测定地质化探样品中金[J].冶金分析, 2016, 36(7):34-38. http://d.old.wanfangdata.com.cn/Periodical/yjfx201607005
    [11]
    李先和, 万双.火试金富集-电感耦合等离子体质谱法(ICP-MS)测定铜渣尾矿中的金含量[J].中国无机分析化学, 2015, 5(4):79-82. doi: 10.3969/j.issn.2095-1035.2015.04.018
    [12]
    单兴刚, 林云芬.乙酸丁酯萃取-火焰原子吸收光谱法测定矿石中痕量金[J].冶金分析, 2011, 31(3):64-67. doi: 10.3969/j.issn.1000-7571.2011.03.013
    [13]
    张灏宇.活性炭吸附原子吸收光谱法测定含镍物料中金[J].冶金分析, 2005, 25(5):86-87. http://d.old.wanfangdata.com.cn/Periodical/yjfx200505024
    [14]
    唐良保.原子吸收光谱法快速测定地质样品中痕量金[J].国外铀金地质, 1999, 16(1):94-96. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=QK199900175577
    [15]
    刘溢锋, 冯俊汉, 李展江, 等.电感耦合等离子体发射光谱法同时测定粗铜中的金和银[J].冶金分析, 2012, 32(7):52-54. doi: 10.3969/j.issn.1000-7571.2012.07.011
    [16]
    李瑞仙, 巨力佩, 黑文龙, 等.电感耦合等离子体发射光谱法测定锑金精矿中的金[J].甘肃地质, 2012(4):77-81. http://d.old.wanfangdata.com.cn/Periodical/hggl201732104
    [17]
    王景凤.火试金富集测定粗铅中金、银含量的改进试验研究[J].有色金属科学与工程, 2018, 9(3):100-104. http://ysjskx.paperopen.com/oa/darticle.aspx?type=view&id=201803017
    [18]
    梁金凤, 王景凤.火试金重量法测定铅阳极泥中银含量方法的改进[C]∥2014国际冶金及材料分析测试学术报告会论文集, 北京: 中国金属学会, 2014, 34: 314-317.
    [19]
    王景凤.火试金重量法测定金精矿中金银含量方法的改进[J].有色矿冶, 2007, 33(1):58-60.
    [20]
    李宗林.活性炭吸附-碘量法测定金[J].有色矿冶, 1991(5):45-47. http://d.old.wanfangdata.com.cn/Periodical/huangj200911015
    [21]
    李国先, 柏云巧.提高火试金法进行金精矿含金量测定可操作性的探讨[J].山东工业技术, 2015(12):42. http://d.old.wanfangdata.com.cn/Periodical/sdgyjs201512037
    [22]
    中华人民共和国国家标准.GB/T 7739.1-2007金精矿化学分析方法第1部分: 金量和银量的测定火法冶炼[S].北京: 中华人民共和国国家发展和改革委员会, 2007.
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