工艺参数对引晶法制备半固态浆料组织的影响

Influence of process parameters on semi-solid slurry prepared by introducing grain process

  • 摘要: 采用引晶法(Introducing Grain Process,简称IGP)制备半固态金属浆料,研究了工艺参数对半固态A356铝合金浆料组织的影响,讨论了球状初生α(Al)晶粒的形成机制及形貌控制.结果表明:当合金温度为630 ℃、制备浆料为4 kg时,如果引晶尺寸为10 mm、加入量为3.5 %(质量分数)和倾倒温度为611~617 ℃,半固态浆料中初生α(Al)晶粒的平均直径可达40~75 μm,形状因子可达0.82~0.89.如果引晶尺寸为10 mm、倾倒温度为613 ℃、加入量为2 %~4 %,初生α(Al)晶粒的平均直径可达45~ 82 μm,形状因子可达0.78~0.88.合金温度和倾倒温度适当降低、或者引晶加入量适当提高,组织越好.当QR =QA、Rh= Rc时,只要倾倒温度适宜就可以制备优质半固态浆料.引晶熔化时产生的枝晶碎块是半固态浆料中初生α(Al)晶粒的直接来源,引晶熔化时形成的温度过冷区也为异质形核提供了有利条件.

     

    Abstract: Semi-solid metal slurry was prepared by introducing grain process (IGP). The influence of the process parameters on microstructures of the semi-solid A356 Al-alloy slurries were investigated, and formation mechanism and morphology controlling of the spherical primary α(Al) grains was discussed. The results show when the alloy temperature is 630 ℃, the preparing slurry is 4 kg, the IG size is 10 mm, dosage is 3.5 % (mass fraction), and dumping temperatures(DTs) are at 611~617 °C, the mean diameters of the primary α(Al) grains in the semi-solid slurries can reach 40~75 μm and the shape factors can reach 0.82~0.89. When the IG size is 10 mm, the DT is at 613 ℃, and dosage is 2 %~4 %, the mean diameters can reach 45~82 μm and the shape factors can reach 0.78~0.88. With the alloy temperature and the DT decreasing or the dosage increasing properly, the primary α(Al) grain morphology is better. When QR =QA and Rh= Rc, as long as the DT is suitable, excellent semi-solid slurry can be produced. As a result of the IG melting, a large amount of dendritic fragments can become direct source of the primary α(Al) grains. Meanwhile, many under-cooled areas are formed, where abundant primary α(Al) grains are multiplied by heterogeneous nucleation.

     

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